ORIGINAL RESEARCH

The limitations and capabilities of wipe samples analysis in control of contamination of facilities with highly toxic organic compounds

Shachneva MD, Leninskii MA, Savelieva EI
About authors

Research Institute of Hygiene, Occupational Pathology and Human Ecology Leningrad Region, Russia

Correspondence should be addressed: Mariya D. Shachneva
Kapitolovo, r.p. Kuzmolovsky, Vsevolozhsky r., 188663 Leningradskaya obl.; ur.liam@ayiram_avenhcahs

About paper

Author contribution: Shachneva MD — carrying out the experiment, summarizing the results, article authoring and editing; Leninskii MA — carrying out the experiment, article authoring; Savelieva EI — academic advising, article authoring.

Received: 2021-05-28 Accepted: 2021-06-14 Published online: 2021-06-26
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Fig. Extraction efficiency of the target compounds from gauze swabs
Table 1. Detection parameters, sulfur mustard and 1,4-dithiane detected by GC-MS/MS-EI, VR and DEAEMPT by HPLC-MS/MS
Table 2. Matrix factor (%) in detection of sulfur mustard and 1,4-dithiane by GC-MS/MS, VR and DEAEMPT by HPLC-MS/MS, after adding the analytes to the extracts from blank swabs
Таблица 3. Степени извлечения иприта и 1,4-дитиана, VR и ДЭАЭМТФ с различных поверхностей
Note: * — below LOD of 1,4-dithiane (5 × 10–8 mg/dm2)